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The redox activity (Li‐ion intercalation/deintercalation) of a series of individual LiMn2O4 particles of known geometry and (nano)structure, within an array, is determined using a correlative electrochemical microscopy strategy. Cyclic voltammetry (current–voltage curve, I–E) and galvanostatic charge/discharge (voltage–time curve, E–t) are applied at the single particle level, using scanning electrochemical...
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