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A detailed analysis of the IR spectral changes of melt-quenched poly(l-lactic acid) (PLLA) sample is presented. It is found that the glass transition, cold crystallization, disorder-to-order and melting behavior of melt-quenched PLLA can be clearly revealed by choosing suitable characteristic bands and combing the 1st derivative manipulation. Of particular note, it is found that, there are chain segment...
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