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A novel synthetic route toward a macromolecule with linear backbones that bear pendant stable radical groups is described. For this purpose we synthesis a new acrylate tempo monomer (4-acryloyloxy-1-((1-phenylethyl)oxy)-2,2,6,6-tetramethylpiperidine (APEOT)) which is thermally not stable and undergo C-O bond homolysis at higher temperatures accompanied by the generation of radicals. The polymerization...
Cross‐linked poly(ε‐caprolactone) (PCL)‐based polyesterurethane (PUR) systems have been synthesized through Diels–Alder reactions by reactive extrusion. The Diels–Alder and retro‐Diels–Alder reactions proved to be useful for enhancing the molecular motion of PCL‐based systems, and therefore their crystallization ability, in the design of cross‐linked semicrystalline polymers with one‐way and two‐way...
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