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The synthesis of sulfur-containing fluoroacrylic monomers CmF2m+1(CH2)2S(CH2)nOC(O)CHCH2 (where m=6, 8 and n=2–4, 11) is presented from a two-step procedure. The first deals with the radical addition of fluorinated mercaptans CmF2m+1(CH2)2SH onto ω-unsaturated alcohols leading to new ω-perfluorinated alcohols containing various polymethylene spacers CmF2m+1(CH2)2S(CH2)nOH according to the nature of...
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