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Hollandite‐type TiO2 with uniform submicron‐sized particles was prepared using the treatment of K1.2Ti8O16 by KBrO3 in an H2SO4 solution. The electrode material exhibited a 150 mAh g–1 reversible capacity with an average working potential of 1.75 V vs. Li/Li+. Phase transformations taking place during Li+ (de)intercalation were studied by means of synchrotron X‐ray powder diffraction in operando regime...
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