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For the first time a complete solid solution series Ni2xMg2−2xCl(OH)3 of an atacamite type alkaline main group metal chloride, Mg2Cl(OH)3, and a transition group metal chloride, Ni2Cl(OH)3, was prepared and characterized by chemical and thermal analysis as well as by Raman and IR spectroscopy, and high resolution laboratory X-ray powder diffraction. All members of the solid solution series crystallize...
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