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Two samples of pure NiCl(OH) were produced by hydrothermal synthesis and characterized by chemical analysis, IR spectroscopy, high‐resolution laboratory X‐ray powder diffraction and scanning electron microscopy. Layers composed of edge‐sharing distorted NiCl6x(OH)6−6x octahedra were identified as the main building blocks of the crystal structure. NiCl(OH) is isostructural to CoOOH and crystallizes...
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