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A mixed lead/tin bromide carbodiimide oxide was synthesized by solid‐state reaction between Pb(CN2), PbBr2, SnBr2 and SnO at 400 °C. Its monoclinic crystal structure was solved and refined in the space group C2/m by single‐crystal X‐ray diffraction from a yellow single crystal. One crystallographic site was found to be occupied by both tin and lead, in agreement with the results of energy‐dispersive...
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