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GdAuMg was synthesized by reaction of the elements in a sealed tantalum ampule in a high-frequency furnace. The structure was investigated by X-ray diffraction on both powders and single crystals: ZrNiAl type, P62m, a=756.3(1), c=412.71(7) pm, wR2=0.0285 for 308 F 2 values, 14 variables. Geometrical motifs of the GdAuMg structure are gold centered tricapped trigonal prisms [Au1Mg 3 ...
Pure samples of CaPdSn, CaPtSn, SrPtSn, SrAuSn and BaAuSn can be prepared by reacting the elements in glassy carbon crucibles or in sealed tantalum tubes in a water-cooled sample chamber of a high-frequency furnace. The stannides have been investigated by X-ray diffraction on powders. Single crystal data yielded: TiNiSi type, Pnma, a=764.16(7), b=470.74(4), c=799.64(7) pm, wR 2 =0.0622, 469<space>F...
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