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Black shiny platelets of Bi8Pt5I3 and Bi16Pt11I6 were crystallized from melts of the metals and BiI3. Despite very similar compositions and close peritectics, a protocol for targeted synthesis could be developed based on differences of the decomposition pressures. Bi8Pt5I3 has a monoclinic crystal structure [space group C2/m; a = 1850.7(2) pm, b = 391.46(3) pm, c = 1340.5(1) pm, β = 113.28(1)°], in...
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