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Illumination-assisted droplet spray ionization (IA-DSI) mass spectrometry was developed for in situ analysis and real-time monitoring of photolysis reactions. In IA-DSI, a photolysis reaction occurs on a corner of a cover slip positioned in front of a mass spectrometer, and the generated reaction intermediates are ionized via the corner and are directed to the inlet and analyzed by a mass spectrometer...
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