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The titled materials were obtained neutralizing in situ prepared aqueous solutions of H3[M(CN)6] (M = Fe, Co) by adding Mg(OH)2 and evaporating the solvent under vacuum. Their crystal structure was solved and refined from powder X‐ray diffraction data. The two solids crystallize with a cubic unit cell, in the Pm$\bar{3}$m space group, which corresponds to an ordered distribution of [M(CN)6] vacancies...
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