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The commercialization of MXenes as anodes for lithium‐ion batteries is largely impeded by low initial coulombic efficiency (ICE) and unfavorable cycling stability, which are closely associated with defects such as Ti vacancies (VTi) in Ti3C2 MXenes. Herein, an effective strategy is developed to deactivate VTi defects by in situ growing Al2O3 nanoclusters on MXenes to alleviate the irreversible electrolyte...
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