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The preparation and isolation of 5,5′-bis(2-hydroxytetrazole) by oxidation of 5,5′-bistetrazole using commercially available oxone is described. The nitrogen-rich salts including ammonium, hydroxylammonium, guanidinium, aminoguanidinium, triaminoguanidinium, 5-aminotetrazolium and aminonitroguanidinium have been prepared, characterized (XRD, NMR and vibrational spectroscopy, DSC, mass spectrometry)...
The energetic nitrogen-rich compounds 1,3-bis(1-methyltetrazol-5-yl)triaz-1-ene (4) and 1,3-bis(2-methyltetrazol-5-yl)triaz-1-ene (5) were synthesized by diazotation of 1-methyl-5-aminotetrazole (2) and 2-methyl-5-aminotetrazole (3), respectively, by using half an equivalent of sodium nitrite. The reaction of 4 and 5 with diluted ammonia solution yields ammonium bis(1-methyltetrazol-5-yl)triazenate...
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