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A Dynamic Nuclear Polarisation (DNP) enhanced solid-state Magic Angle Spinning (MAS) NMR spectrometer operating at 6.7T is described and demonstrated. The 187GHz TE 13 fundamental mode of the FU CW VII gyrotron is used as the microwave source for this magnetic field strength and 284MHz 1 H DNP-NMR. The spectrometer is designed for use with microwave frequencies up to 395GHz (the TE...
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