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TiAl3 intermetallic has been successfully synthesized by the electrochemical deoxidation of the Ti/Al-containing oxides precursors including TiO2/Al2O3 mixture and titanium-rich slag/Al2O3 mixture at 1000 °C and 3.8 V in molten CaCl2. A solid oxide membrane (SOM) tube filled with carbon-saturated liquid tin was served as inert anode, and the pressed pellet of Ti/Al-containing oxides precursors was...
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