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A reactive amphiphile, SA1, which comprises a mercaptodecyl oleophilic tail and a β-alanine oleophobic moiety, has been introduced to serve as the building block for supramolecular filler. At least a fraction of SA1 reacts in situ during mechanically mixing and vulcanization with SBR via thiol-ene reaction. Some oxidative dimerization also concomitantly occurs to give DSA1. The chemical coupling between...
A strategy of supramolecular reinforcement of elastomers is conceptualized and demonstrated. Amphiphile A consisting of a β-alanine oleophobic motif and a pentadecyl oleophilic motif is designed to self-assemble in a continuous rubber phase to form discrete micelle-type structures under high-temperature processing conditions and crystallize upon cooling to form supramolecular reinforcing particles...
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