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PurposeA resonance at ∼181 ppm in the 13C spectra of tumors injected with hyperpolarized [U‐2H, U‐13C]glucose was assigned to 6‐phosphogluconate (6PG), as in previous studies in yeast, whereas in breast cancer cells in vitro this resonance was assigned to 3‐phosphoglycerate (3PG). These peak assignments were investigated here using measurements of 6PG and 3PG 13C‐labeling using liquid chromatography...
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