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Lead‐containing plexiglass is prepared successfully via copolymerization of lead‐methacrylate (Pb(MAA)2 and the acrylic monomer such as methyl methacrylate, methyl acrylate, ethyl acrylate, and butyl acrylate. The results show that as‐prepared plexiglass has good photons shielding performance and resistance to the discoloration induced by radiation (10 kGy γ‐ray), and the alteration of shielding performance...