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Hierarchical core–shell Fe3O4@Mg3Al–CO3 layered double hydroxide (LDH) as an efficient magnetic adsorbent was prepared and investigated for the adsorption of anionic dye under ambient conditions. The material was thoroughly characterized by a variety of spectroscopic methods, which indicate that it was composed of spherical Fe3O4 (ca. 330 nm) core with a vertically aligned Mg3Al‐CO3 layered double...
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