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3D printing changes the scope of how samples can be mounted for small‐angle X‐ray scattering (SAXS). In this paper a 3D‐printed X‐ray chamber, which allows for in situ exchange of buffer and in situ optical transmission spectroscopy, is presented. The chamber is made of cyclic olefin copolymers (COC), including COC X‐ray windows providing ultra‐low SAXS background. The design integrates a membrane...