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High-molecular-weight bulky-block poly(fluorenyl ether thioether ketone)s were successfully synthesized by a two steps one-pot protocol using N,N′-dimethy-S-carbamate masked dithiols for vanadium redox flow battery (VRB) application. The followed sulfonation procedure gave birth to novel sulfonated block poly(fluorenyl ether thioether ketone)s (SPFETKs) with controlled ionic exchange capacities (IEC)...
A novel fluorene-containing poly(arylene ether ketone) were synthesized followed by sulfonating into a series of sulfonated fluorene-containing poly(arylene ether ketone)s using chlorosulfonic acid. The sulfonated polymers were thereafter cast into membranes from their solutions. The properties of the ionic exchange capacity, sulfonation degree, water-uptake, mechanical properties, thermal and oxidative...
In this paper, graphite/polystyrene nanocomposite is synthesized by in situ polymerization of styrene in a tetrahydrofuran (THF) solution system of potassium (K)–THF–graphite intercalation compound (GIC). K–THF–GIC has proved to initiate polymerization of styrene by the anionic mechanism. Due to the interfacial interaction between the graphite nanolayers and the polymer, the composites exhibit higher...
A composite based on exfoliated graphite (EG) and polystyrene was prepared by a polymerization-filling technique. With augmentation of filled EG, the molecular weight of polystyrene in the resulting composite increased and the molecular weight distribution decreased. The glass transition temperature of the polystyrene was determined by dynamic mechanical analysis (DMA) and showed that it increases...
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