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LiCaAlN2:Eu3+/Tb3+ red/green phosphors were successfully prepared by conventional solid‐state reaction. The photoluminescence (PL) properties and cathodoluminescence (CL) properties of LiCaAlN2:Eu3+/Tb3+ were investigated in detail. The Eu3+ (Tb3+) doped LiCaAlN2 shows red (green) emission peaking at 615 nm (550 nm). Monitored at 615 nm (550 nm), it is interesting to found that LiCaAlN2:Eu3+ (LiCaAlN...
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