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Nitrogen-containing carbon was prepared from the vapor deposition of acetonitrile at 900 °C over silica- or magnesia-supported Fe, Co, and Ni particles. The byproducts of pyrolysis were monitored by mass spectrometry. The carbon formed from silica precursors was washed with KOH to remove the silica and HCl to remove metal particles, whereas the carbon formed from magnesia samples was washed with HCl...
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