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The reasonable design of the precursor of a carbon‐based nanocatalyst is an important pathway to improve catalytic performance. In this study, a simple solvothermal method was used to synthesize [Cu(TPT)(2,5‐tdc)] ⋅ 2H2O (Cu‐MOF), which contains N and S atoms, in one step. Further in‐situ carbonization of the Cu‐MOF as the precursor was used to synthesize Cu/CuxS‐embedded N,S‐doped porous carbon (Cu/Cu...
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