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GdBaCo 2−x Ni x O 5+δ (x = 0–0.8) cathode materials have been synthesized by a citrate-gel modified chemical route, by which we have achieved a high level of substitution up to x = 0.8. Oxygen stoichiometry at room temperature has been determined by iodometry and the structural evolution as a function of Ni content has been extracted from XRD patterns analysis. All compounds...
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