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The unprecedented co‐thermolysis of decaborane(14) (nido‐B10H14) and toluene results in a novel porous material (that we have named “activated borane”) containing micropores between 1.0 and 1.5 nm in diameter and a specific surface area of 774 m2 g−1 (Ar, 87 K) that is thermally stable up to 1000 °C. Solid state 1H, 11B and 13C MAS NMR, UV‐vis and IR spectroscopies suggest an amorphous structure of...
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