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Nickel‐based electrocatalysts are promising candidates for oxygen evolution reaction (OER) but suffer from high activation overpotentials. Herein, in situ structural reconstruction of V‐doped Ni2P pre‐catalyst to form highly active NiV oxyhydroxides for OER is reported, during which the partial dissolution of V creates a disordered Ni structure with an enlarged electrochemical surface area. Operando...
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