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The new compound (TeI3)2[W6I14] appeared as an unforeseen product from a reaction of WTe2 with iodine at 250 °C, representing an exceptionally low temperature for the formation of an octahedral tungsten iodide cluster. The crystal structure, as refined by single‐crystal X‐ray diffraction, reveals (TeI3)+ ions and the well‐known [W6I14]2– cluster. A chemical analysis confirms the identity of the product...
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