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In this paper, magnetic mesoporous silica microspheres with C8‐modified interior pore‐walls were prepared through a facile one‐pot sol–gel coating strategy, and were successfully applied for selective enrichment of endogenous peptides in mouse brain for peptidome analysis. Through the one‐pot sol–gel approach with surfactant (CTAB) as a template, tetraethyl orthosilicate (TEOS) and n‐ctyltriethoxysilane...
In this work, we report the development of a novel enrichment protocol for peptides by using the microspheres composed of Fe3O4@nSiO2 Core and perpendicularly aligned mesoporous SiO2 shell (designated Fe3O4@nSiO2@mSiO2). The Fe3O4@nSiO2@mSiO2 microspheres possess useful magnetic responsivity which makes the process of enrichment fast and convenient. The highly ordered nanoscale pores (2 nm) and high‐surface...
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