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A combined scanning microelectrochemical procedure is proposed to obtain information on the action of corrosion inhibitors on metals. The method uses the scanning vibrating electrode technique (SVET) and the scanning electrochemical microscopy (SECM). Antimony tips are employed as the sensing probe in SECM, allowing this technique to be operated in both potentiometric and amperometric modes. This...
A new method for the spatially resolved measurement of pH during corrosion processes with the scanning electrochemical microscope (SECM) is presented. Antimony tips are employed because the dual-function characteristics of this material allow the combined amperometric/potentiometric operation of the SECM. The applicability of this technique is illustrated by considering the galvanic corrosion of a...
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