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The reaction between trans-PhPdI(PPh 3 ) 2 and EtO 2 C–CCH has been investigated. This carbopalladation step involved in palladium-catalyzed multicomponent reactions with alkynes gives the unusual trans-adduct EtO 2 C–C(PdIL 2 )CHPh 1 as the major complex formed by isomerization of the primary cis-adduct EtO 2 C–C(PdIL 2 )CHPh 2. The carbopalladation...
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