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Synthesis of the disaccharide β-d-Glup-(1→3)-6-deoxy-α-l-Talp II, and its dimer III from the O-antigenic polysaccharide of Burkholderia pseudomallei strain 304b, were achieved through assembly of suitably synthesized building blocks, 4-methoxylphenyl 6-deoxy-2,4-di-O-benzoyl-α-l-talopyranoside (7), 3-O-allyl-2,4,6-tri-O-benzoyl-α,β-d-glucopyranosyl trichloroacetimidate (8) and 2,3,4,6-tetra-O-benzoyl-α,β-d-glucopyranosyl...
An efficient synthesis of α-d-GlcpNAc-(1→2)-[α-d-ManpNAc-(1→3)-]α-l-Rhap-(1→2)-α-l-Rhap-(1→3)-α-l-Rhap (1), the repeating unit of the O10 antigen from Acinetobacter baumannii was achieved via sequential assembly of the building blocks, p-methoxylphenyl 2,4-di-O-benzoyl-α-l-rhamnopyranoside (2); 2-O-allyloxycarbonyl-3,4-di-O-benzoyl-α-l-rhamnopyranosyl trichloroacetimidate (3); 4-methoxylphenyl 3-O-allyloxycarbonyl-4-O-benzoyl-α-l-rhamnopyranoside...
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