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The intermetallic phase SrNi2–xSb2 was synthesized by arc melting mixtures of the elements and subsequent annealing under argon, and its structure was investigated by means of both powder and single‐crystal X‐ray diffraction methods. It crystallizes with the ThCr2Si2 type (tI10, I4/mmm) and has a homogeneity range of x = 0.15(1)–0.28(1), which does not include the exact stoichiometric 1:2:2 composition...
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