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New indides, Nd 3 Ge 1.18 In 0.82 and Sm 3 Ge 1.33 In 0.67 , were synthesized from the elements by arc-melting and subsequent annealing at 870 K. Single crystals were grown through special annealing procedures in sealed tantalum tubes in a resistance furnace. Both compounds were investigated on the basis of X-ray powder and single crystal data: La ...
The binary intermetallic compound Mg 2+x Ir 3−x was prepared by reacting the elements under reduced argon pressure in a tantalum crucible at 1500 K followed by slow cooling. Repeated grinding, pressing and heating is necessary to get pure samples. The structure of Mg 2 Ir 3 was investigated by X-ray diffraction on both powders and single crystals: V 2 (Co ...
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