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The synthesis and characterisation of a library of acyclic antimony(III) and bismuth(III) triaryl pnictogen bonding (PnB) receptor systems are reported. In the first‐generation receptor series, quantitative 1H NMR chloride titration experiments in THF solvent media reveal halide anion binding potency is intimately correlated with both the electronic‐withdrawing nature of the aryl‐ substituent and...
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