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Phenyl groups were introduced at the β‐positions proximal to the meso‐hydroxy moiety in hydroxyporphyrin NiII complexes by oxidized BINAP PdII complexes. Ion‐pairing assemblies of deprotonated π‐electronic anions, anionic site of which was stabilized by the introduced phenyl moieties with a bulky cation, were formed. They showed charge‐by‐charge assemblies, assembly modes of which were modulated by...
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