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Reaction of [PPN][HFe(CO)4] (PPN = bis(triphenylphosphine)iminium) with PCl3 in a 1:1 ratio produced small amounts of [PPN][P{Fe(CO)4}2Cl2] ([PPN][Ia]). Reaction of [Et4N][HFe(CO)4] with AsCl3 in a 1:0.75 ratio in THF at −78 °C produced [Et4N][As{Fe(CO)4}2Cl2] ([PPN][Ib]) as the majority product. The compound [PPN][(CO)4FePCl2O] ([PPN][II]) was obtained from the reaction of Fe2(CO)9 with PCl3 in THF...
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