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The divalent cobalt complex of the diprotic pincer ligand bis‐pyrazolylpyridine, (H2L)CoCl2, is dehydrohalogenated twice by LiN(SiMe3)2 in the presence of PEt3 to give monomeric S=1/2 LCo(PEt3)2 (1), fully characterized in the solid‐state and solution as a square pyramidal monomer with a long axial Co−P bond. This 17‐electron species reacts in time of mixing with N2O to form L2Co2(μ‐OPEt3) (2)+3 OPEt...
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