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Design and fabrication of low-cost, high efficient and robust three-dimensional (3D) microspherical materials for energy conversion and storage is of paramount importance. Here, we first reported a template-free and efficient hydrothermal method to synthesize quaternary AgPb10SbTe12 (AgPbmSbTem+2, m=10) microspheres comprised of tiny nanoparticles driven by co-doping synergetic dipole-driven aggregation...
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