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The rhodium complex [Rh(Ph2PCH2CH2CH2PPh2)(η6‐FC6H5)][BArF4], 2, catalyzes BH/BD exchange between D2 and the boranes H3B⋅NMe3, H3B⋅SMe2 and HBpin, facilitating the expedient isolation of a variety of deuterated analogues in high isotopic purities, and in particular the isotopologues of N‐methylamine‐borane: R3B⋅NMeR21‐dx (R=H, D; x=0, 2, 3 or 5). It also acts to catalyze the dehydropolymerization...
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