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Redox‐inactive metal ions play important roles in tuning chemical properties of metal–oxygen intermediates. Herein we report the effect of water molecules on the redox properties of a nonheme iron(III)–peroxo complex binding redox‐inactive metal ions. The coordination of two water molecules to a Zn2+ ion in (TMC)FeIII‐(O2)‐Zn(CF3SO3)2 (1‐Zn2+) decreases the Lewis acidity of the Zn2+ ion, resulting...
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