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New couple: A cross‐coupling reaction at the carbon vertex of a monocarba‐closo‐dodecaborate has been developed to allow efficient introduction of various aryl groups and other sp2/sp‐hybridized carbon centers. A copper(I) complex facilitated the coupling process with a wide range of electrophiles at room temperature. The reaction was used to prepare a series of C‐arylated carborane anion derivatives...
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