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Bis[2‐(4‐bromopyrazol‐1‐yl)ethyl] disulfide and diselenide L1 and L2 were synthesized by the reactions of 4‐bromo‐1‐(2‐chloroethyl)‐1H‐pyrazole with the in situ generated Na2S2 and Na2Se2. The reactions of L1 and L2 with 2 equiv. of [PdCl2(CH3CN)2] in CH3CN at 70 °C proceed through an oxidative addition/reductive elimination sequence to the PdII center to form the chalcogenolato‐bridged dinuclear...
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