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Developing photocatalysts with excellent H2 evolution performance has been an urgent concern for practical application. Herein, Ni‐doped Mn0.5Cd0.5S was prepared using one‐step alkaline hydrothermal strategy. Investigation shows that doping Ni element can enhance the performance of Mn0.5Cd0.5S. 3% Ni‐doped Mn0.5Cd0.5S can obtain the highest rate at 108.3 mmol g−1 h−1 (λ > 420 nm), and nearly 14...
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