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Acyclic conformational control often relies on destabilising noncovalent interactions to give rise to predictable conformer populations. Pertinent examples of such strategies include allylic strain (A1,2 and A1,3) and syn‐pentane interactions. However, the incorporation of fluorine vicinal to an electron‐withdrawing group (F–Cβ–Cα–X) can lead to predictable conformations as a consequence of stabilising...
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