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A novel 3D copper(I) coordination polymer [Cu8(ptim)8·3CH3CH2OH·2H2O] with the ligand 2,4,5‐tri(4‐pyridyl)‐imidazole (Hptim) was synthesized and characterized. During the reaction, Hptim is oxidized by copper(II) and loses its hydrogen atom from the imidazole ring to add one coordination position. The novel complex has a 3D pillared double‐layer network. The topological analysis of the crystal structure...
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