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The reaction of {(HNEt3)2[Ag10(tBuC6H4S)12]}n, Ag2O, Na2MoO4, and m‐methoxybenzoic acid (Hmbc) in CH3OH/CH2Cl2 led to yellow crystals of [Ag4S4 (MoO4)5@Ag66] (SD/Ag70b; SD=SunDi) only, while in the presence of DMF, additional dark‐red crystals of [Ag10@ (MoO4)7@Ag60] (SD/Ag70a) were obtained. SD/Ag70b consists of five MoO42− ions wrapped by a shell of 66 Ag atoms, while SD/Ag70a contains a rare Ag...
Der Aufbau von Silber‐Nanoclustern mit Schalenstruktur lässt sich durch Lösungsmittel modulieren. In ihrer Zuschrift auf S. 6342 nutzen D. Sun et al. Anionen‐Template und Lösungsmittelstrategien in der Synthese von zwei hierarchischen dreilagigen Silber‐Nanoclustern. Der Ag10‐Kern, welcher aus fünf verbundenen Ag4‐Tetraedern besteht, repräsentiert dabei eine neue embryonische Silberspezies in der...
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