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In this study, free Ti/Si/Al/C powder mixtures with molar ratios of 3:0.8:0.4:1.8 were heated in argon with various schedules, in order to reveal the possibility for the synthesis of high Ti 3 Si 0.8 Al 0.4 C 1.8 content powder. X-ray diffraction (XRD) was used for the evaluation of phase identities of the powder after different treatments. Scanning electron microscopy...
Ti/Sn/TiC powder mixtures were first employed to synthesize Ti 2 SnC powder by pressureless sintering in the temperature range of 950–1250 °C at vacuum atmosphere. Ti 2 SnC began to form at 950 °C, its content increased with increasing temperature. High purity of Ti 2 SnC was obtained by sintering the mixtures with deficient Sn and TiC at 1200 °C for 15 min. A reaction mechanism...
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