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Separation of linear and branched isomers is of great commercial significance but still one of the energy‐intensive and challenging processes in petrochemical industry. Here, we for the first time report a tailor‐made metal–organic framework, ZU‐36‐Co (also termed GeFSIX‐3‐Co, GeFSIX = GeF62−, 3 = pyrazine), for the separation of both C4 linear/branched olefins (n−/iso‐C4H8) and paraffin isomers (...
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